This course introduces participants to the principles and applications of Scanning Electron Microscopy (SEM) and Energy Dispersive X-ray Spectroscopy (EDS) for surface imaging and elemental analysis. It covers instrument components, sample preparation, imaging techniques, and data interpretation. Participants will learn how SEM provides high-resolution surface morphology and how EDS complements it by identifying elemental composition. Hands-on sessions are included to reinforce practical understanding and operation.